Elsevier

Journal of Endodontics

Volume 29, Issue 11, November 2003, Pages 751-755
Journal of Endodontics

BASIC RESEARCH-TECHNOLOGY
Radiopacity of Endodontic Sealers: Development of a New Method for Direct Measurement

https://doi.org/10.1097/00004770-200311000-00016Get rights and content

Radiopacity is an essential attribute of endodontic filling materials. It is important to see clearly the root canal filling to detect its presence, extent, and apparent condensation. National and international standards require a minimal radiopacity equivalent to 3 or 4 mm of aluminum, yet some products made by reputed companies do not meet this requirement. The result may be unjustified downgrading of clinical cases. The purpose of this investigation was 2-fold: to develop a novel and easily reproducible technique for assessing the radiopacity of endodontic sealers and to apply it to measure the opacity of 21 current cements poured in 6- × 1-mm wells. As in the currently recommended technique, the standardized samples are radiographed alongside an aluminum stepwedge but instead of using an optical densitometer to measure the density and then calculate the radiopacity, the image is digitized. The gray pixel value of the test material is compared with the stepwedge, using computer software, to find the corresponding step. The opacity of the samples ranged from 1.6 mm to more than 11 mm of aluminum. The technique can be advanced to a dry, chemical-less variant by using radiation captors, as for periapical X-rays, instead of film.

Section snippets

Sample Preparation

The list of endodontic sealers to be tested was compiled from the current literature and from commercial advertisement brochures (Table 1). The test materials were purchased from local suppliers and if they were not available, the manufacturer was kindly requested to send two packages of sealer from the current batch for an investigation of its physical properties. The materials were mixed in accordance with the manufacturers’ instructions whenever available and poured in a freshly mixed state

RESULTS

The empty background (including the glass carrier) gave a reading of 8 to 15 pixels. The graph constructed by plotting the number of pixels exhibited by the first 12 steps in the film against the aluminum thickness (in mm) of the step yielded a practically straight line. A new line was drawn, parallel to the first but 12 pixels lower to account for the mean base and fog of the film (Fig. 3). In view of its quasi linearity, it was possible to determine by extrapolation the radiopacity of the

DISCUSSION

The results are difficult to compare with those of previous studies of the radiopacity of endodontic sealers because only one (3) expressed the radiopacity of aluminum in mm, but the long list of tested materials contains few contemporary sealers. The radiopacity of those that are still in use tends to be similar to the presently measured value, albeit slightly lower: AH 26 only 6.66, Roth’s 801 sealer 4.41, versus 5.1. The other zinc-oxide-eugenol–based sealers without potent opacifiers such

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